Buch, Deutsch, Band 784, 145 Seiten
Reihe: Vefahrenstechnik
Catalytic distillation, the combination of heterogeneously catalysed reaction and multistage distillation, is one of the most important applications of the reactive separation process concept. In this thesis, a general analysis of steady-state and dynamic catalytic distillation processes is presented, encompassing model development, simulation as well as experimental studies. Experiments conducted in this thesis cover model parameter identification, such as reaction kinetics and hydrodynamics of catalytic packings, as well as transient catalytic distillation experiments. Simulation studies were conducted for two different catalytic distillation systems, namely the synthesis of methyl acetate and the synthesis of diethyl carbonate. Based on sensitivity studies this work answers the questions of optimum model complexity with regard to mass transfer, chemical reaction and non-ideal flow behaviour.
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