Two-Dimensional NMR Methods for Establishing Molecular Connectivity

A Chemist's Guide to Experiment Selection, Performance, and Interpretation
1. Auflage 1988
ISBN: 978-0-471-18707-3
Verlag: Wiley

Buch, Englisch, 528 Seiten, Format (B × H): 161 mm x 240 mm, Gewicht: 953 g

This guide to two-dimensional NMR spectroscopy helps the novice who want e the technique, but needs a path through the bewildering array of metho acronyms and the mathematical rigor found in most books.
The authors provide a clear explanation of experiment performance, param lection, data processing and presentation as well as a description of wh rmation is provided by each experiment and how it is extracted and inter They group presentations of two-dimensional NMR experiments according t zation, e.g. COSY, LRCOSY, ZQCOSY, DQCOSY. for establishing proton-pr nnectivities.
The book also presents spectra of the same model compound using various ues to enable the reader to make direct comparisons and facilitate his e nt selection. Examples of the concerted utilization of various two-dimen NMR experiments to solve complex structural problems are also given.

Zielgruppe

Studenten höherer Semester, Organiker, Physikochemiker, Laboratorien, analytische, Bibliotheken

Autoren/Hrsg.

Martin, G E

Zektzer, A S

Fachgebiete

• Naturwissenschaften Physik Quantenphysik Atom- und Molekülphysik
• Naturwissenschaften Chemie Analytische Chemie Massenspektrometrie, Spektroskopie, Spektrochemie

Inhaltsverzeichnis

Introduction and Practical Considerations of Two-Dimensional NMR Spectroscopy.

Heteronuclear Chemical shift Correlation.

Relayed Coherence Transfer and Related 2D-NMR Experiments.

13_C-13_C Double Coherence 2D-NMR. The Inadequate Experiments.

Applications Problems.

Solutions to Problems.

Index.