Practical Guide to ICP-MS

A Tutorial for Beginners, Third Edition
3. Auflage 2013
ISBN: 978-1-4665-5543-3
Verlag: Taylor & Francis Inc

Buch, Englisch, 446 Seiten, Format (B × H): 159 mm x 241 mm, Gewicht: 742 g

Reihe: Practical Spectroscopy

Written by a field insider with over 20 years experience in product development, application support, and field marketing for an ICP-MS manufacturer, the third edition of Practical Guide to ICP-MS: A Tutorial for Beginners provides an updated reference that was written specifically with the novice in mind. It presents a compelling story about ICP-MS and what it has to offer, showing this powerful ultra trace-element technique in the way it was intended—a practical solution to real-world problems.

New to the third edition:

- New chapter: Emerging ICP-MS Application Areas – covers the three most rapidly growing areas: analysis of flue gas desulfurization wastewaters, fully automated analysis of seawater samples using online chemistry procedures, and characterization of engineered nanoparticles

- Discussion of all the new technology commercialized since the second edition.

- An updated glossary of terms with more than 100 new entries

- Examination of nonstandard sampling accessories, which are important for enhancing the practical capabilities of ICP-MS

- Insight into additional applications in the environmental, clinical/biomedical, and food chemistry fields as well as new directives from the United States Pharmacopeia (USP) on determining impurities in pharmaceuticals and dietary supplements using Chapters <232>, <233> and <2232>

- Description of the most important analytical factors for selecting an ICP-MS system, taking into consideration more recent application demands

This reference describes the principles and application benefits of ICP-MS in a clear manner for laboratory managers, analytical chemists, and technicians who have limited knowledge of the technique. In addition, it offers much-needed guidance on how best to evaluate capabilities and compare with other trace element techniques when looking to purchase commercial ICP-MS instrumentation.

Zielgruppe

Professional Practice & Development

Autoren/Hrsg.

Thomas, Robert

Fachgebiete

• Naturwissenschaften Chemie Analytische Chemie Massenspektrometrie, Spektroskopie, Spektrochemie

Inhaltsverzeichnis

An Overview of ICP-MS. Principles of Ion Formation. Sample Introduction. Plasma Source. Interface Region. Ion-Focusing System. Mass Analyzers: Quadrupole Technology. Mass Analyzers: Double-Focusing Magnetic Sector Technology. Mass Analyzers: Time-of-Flight Technology. Mass Analyzers: Collision/Reaction Cell and Interface Technology. Ion Detectors. Peak Measurement Protocol. Methods of Quantitation. Review of Interferences. Sample Preparation. Routine Maintenance. Alternative Sample Introduction Techniques. Coupling ICP-MS with Chromatographic Techniques for Trace Element Speciation. Common ICP-MS Applications. Emerging ICP-MS Application Areas. Comparing ICP-MS with Other Atomic Spectroscopic Techniques. How to Select an ICP Mass Spectrometer: Some Important Analytical Considerations. Final Thoughts. Useful Contact Information. Glossary of ICP-MS Terms. References. Index.

Über Autor(innen)

Robert J. Thomas, GRIC, FRSC is principal of Scientific Solutions, a consulting company based in Gaithersburg, Maryland, that serves the application, training, and technical writing needs of the trace element analysis user community. He has worked in the field of atomic spectroscopy (AS) for almost 40 years, with over 20 years’ experience in ICP-MS applications, product development, and sales and marketing support at Perkin Elmer Instruments, Inc. He has written more than 80 technical publications covering a wide variety of atomic spectroscopic subject matter, from the fundamental principles of the technique, to articles solving real-world application problems with AA, ICP-OES, and ICP-MS analytical instrumentation.