Elwell / Wood Analysis of the New Metals

Titanium, Zirconium, Hafnium, Niobium, Tantalum, Tungsten and Their Alloys
1. Auflage 2016
ISBN: 978-1-4831-8584-2
Verlag: Elsevier Science & Techn.
Format: PDF
Kopierschutz: 1 - PDF Watermark

E-Book, Englisch, 288 Seiten, Web PDF

Analysis of the New Metals: Titanium, Zirconium, Hafnium, Niobium, Tantalum, Tungsten and their Alloys focuses on methods for the analysis of titanium, zirconium, hafnium, niobium, tantalum, tungsten, and their alloys. Emphasis is on the procedures used in Imperial Metal Industries (Kynoch) Limited's laboratories for the analysis of these metals. These procedures include the oxide-resin procedure, solution procedure, and the point-to-plane spectrographic procedure. Comprised of six chapters, this book begins with an overview of special procedures for obtaining representative samples, including the use of titanium or zirconium sponge (Kroll process) as well as titanium granules (ICI sodium process). Subsequent chapters discuss the identification of titanium and its alloys such as aluminum, boron, calcium, carbon, and copper by means of the point-to-plane spectrographic procedure, a Fuess metal spectroscope, and chemical spot-tests; spectroscopic analysis of zirconium, zirconium alloys, and ionide-refined hafnium; and spectroscopic analysis of niobium, tantalum, tungsten, and their alloys. This monograph will be useful for undergraduate students, educators, practitioners, and researchers in metallurgy.

Autoren/Hrsg.

Elwell, W. T.

Wood, D. F.

Inhaltsverzeichnis

1;Front Cover;1
2;Analysis of The New Metals: Titanium, Zirconium, Hafnium,
Niobium, Tantalum, Tungsten
and their Alloys;4
3;Copyright Page;5
4;Table of Contents;6
5;PREFACE;10
6;ACKNOWLEDGEMENTS;13
7;CHAPTER I. INTRODUCTION;14
7.1;1. SAMPLING;14
7.2;2. GENERAL INFORMATION;17
8;CHAPTER II. TITANIUM AND ITS ALLOYS;22
8.1;3. TYPICAL SPECIFICATIONS (COMPOSITION)— TITANIUM PRODUCTS;22
8.2;4. ALUMINIUM;22
8.3;5. BORON;28
8.4;6. CALCIUM;32
8.5;7. CARBON;33
8.6;8. CHLORINE;41
8.7;9. CHROMIUM;46
8.8;10. COBALT;48
8.9;11. COPPER;52
8.10;12. HYDROGEN;57
8.11;13. IRON;63
8.12;14. MAGNESIUM;64
8.13;15. MANGANESE;75
8.14;16. MOISTURE;78
8.15;17. MOLYBDENUM;80
8.16;18. NICKEL;86
8.17;19. NITROGEN;90
8.18;20. OXYGEN AND HYDROGEN;95
8.19;21. PHOSPHORUS;108
8.20;22. SILICON;111
8.21;23. SILVER;116
8.22;24. SODIUM;117
8.23;25. TIN;122
8.24;26. TITANIUM;124
8.25;27. TUNGSTEN;129
8.26;28. VANADIUM AND CHROMIUM;134
8.27;29. ZINC;137
8.28;30. ZIRCONIUM;139
8.29;IDENTIFICATION OF TITANIUM ALLOYS;143
8.30;31. POINT-TO-PLANE SPECTROGRAPHIC PROCEDURE;143
8.31;32. USING A FUESS METAL SPECTROSCOPE;145
8.32;33. CHEMICAL SPOT-TESTS;149
9;CHAPTER III. ZIRCONIUM, HAFNIUM AND THEIR ALLOYS;151
9.1;34. TYPICAL ANALYSIS OF ZIRCONIUM, ZIRCONIUM ALLOYS AND HAFNIUM IONIDE-REFINED;151
9.2;35. ALUMINIUM;152
9.3;36. BORON;155
9.4;37. CADMIUM;160
9.5;38. CALCIUM;164
9.6;39. CARBON;168
9.7;40. CHLORINE;168
9.8;41. CHROMIUM;169
9.9;42. COBALT;171
9.10;43. COPPER AND MOLYBDENUM;174
9.11;44. HYDROGEN;177
9.12;45. IRON;177
9.13;46. LEAD;178
9.14;47. LITHIUM;180
9.15;48. MAGNESIUM;183
9.16;49. MANGANESE;183
9.17;50. MOLYBDENUM AND COPPER;183
9.18;51. NICKEL;185
9.19;52. NIOBIUM;186
9.20;53. NITROGEN;193
9.21;54. OXYGEN AND HYDROGEN;193
9.22;55. PHOSPHORUS;193
9.23;56. SILICON;193
9.24;57. SODIUM;194
9.25;58. TANTALUM;195
9.26;59. TIN AND LEAD;198
9.27;60. TITANIUM;205
9.28;61. TUNGSTEN;206
9.29;62. URANIUM;209
9.30;63. VANADIUM;212
9.31;64. ZINC;213
9.32;SPECTROSCOPIC ANALYSIS OF ZIRCONIUM, ZIRCONIUM ALLOYS AND HAFNIUM;215
9.33;65. IDENTIFICATION OF ZIRCONIUM ALLOYS: USING A FUESS METAL SPECTROSCOPE;217
9.34;66. IDENTIFICATION OF ZIRCONIUM ALLOYS I POINT-TO-PLANE PROCEDURE;218
9.35;67. IMPURITIES IN ZIRCONIUM: POINT-TO-PLANE PROCEDURE;218
9.36;68. IMPURITIES IN ZIRCONIUM! OXIDE-RESIN PROCEDURE;222
9.37;69. BORON, CADMIUM AND LEAD IN ZIRCONIUM: CARRIER-DISTILLATION PROCEDURE;229
9.38;70. RARE EARTHS IN ZIRCONIUM: OXIDE-RESIN PROCEDURE;231
9.39;71. CALCIUM IN ZIRCONIUM! OXIDE-RESIN PROCEDURE;236
9.40;72. IMPURITIES IN HAFNIUM: POINT-TO-PLANE PROCEDURE;237
9.41;73. IMPURITIES IN HAFNIUM: OXIDE-RESIN PROCEDURE;239
9.42;74. ZIRCONIUM IN HAFNIUM: SOLUTION PROCEDURE;242
9.43;75. ZIRCONIUM IN HAFNIUM: POINT-TO-PLANE PROCEDURE;244
9.44;76. ALLOYING CONSTITUENTS IN ZR20: X-RAY FLUORESCENCE PROCEDURE;245
10;CHAPTER IV. NIOBIUM AND ITS ALLOYS;247
10.1;77. TYPICAL SPECIFICATION (COMPOSITION) FOR REACTOR-GRADE NIOBIUM;247
10.2;78. ALUMINIUM;247
10.3;79. BORON;250
10.4;80. CARBON;250
10.5;81. CHROMIUM;250
10.6;82. COPPER AND ZINC;251
10.7;83. HYDROGEN;252
10.8;84. IRON;252
10.9;85. MOLYBDENUM AND TUNGSTEN;255
10.10;86. NICKEL;258
10.11;87. NITROGEN;259
10.12;88. OXYGEN AND HYDROGEN;260
10.13;89. SILICON;260
10.14;90. TITANIUM;261
10.15;91. TUNGSTEN;262
10.16;92. VANADIUM;264
10.17;93. ZIRCONIUM (OR HAFNIUM);264
10.18;SPECTROSCOPIC ANALYSIS OF NIOBIUM;268
10.19;94. IMPURITIES IN NIOBIUM: OXIDE-RESIN PROCEDURE;269
10.20;95. BORON, CADMIUM, LEAD AND TIN IN NIOBIUM: CARRIER-DISTILLATION PROCEDURE
;273
11;CHAPTER V. TANTALUM AND ITS ALLOYS;274
11.1;96. CARBON;274
11.2;97. IRON;274
11.3;98. MOLYBDENUM AND TUNGSTEN;274
11.4;99. NITROGEN;275
11.5;100. OXYGEN AND HYDROGEN;275
11.6;101. ZIRCONIUM;275
12;CHAPTER VI. TUNGSTEN AND ITS ALLOYS;277
12.1;102. BORON;277
12.2;103. CARBON;278
12.3;104. HYDROGEN;278
12.4;105. IRON;278
12.5;106. MOLYBDENUM;278
12.6;107. NICKEL;280
12.7;108. NITROGEN;280
12.8;109. OXYGEN AND HYDROGEN;281
12.9;110. PHOSPHORUS;281
12.10;111. TITANIUM;282
12.11;112. ZIRCONIUM (OR HAFNIUM);282
13;APPENDICES;284
13.1;APPENDIX 1;284
13.2;APPENDIX 2;286
13.3;APPENDIX 3;288
14;INDEX;294