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E-Book

E-Book, Englisch, 276 Seiten

Klotz Techniques in High Pressure Neutron Scattering


Erscheinungsjahr 2013
ISBN: 978-1-4398-3563-0
Verlag: Taylor & Francis
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)

E-Book, Englisch, 276 Seiten

ISBN: 978-1-4398-3563-0
Verlag: Taylor & Francis
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)



Drawing on the author’s practical work from the last 20 years, Techniques in High Pressure Neutron Scattering is one of the first books to gather recent methods that allow neutron scattering well beyond 10 GPa. The author shows how neutron scattering has to be adapted to the pressure range and type of measurement.

Suitable for both newcomers and experienced high pressure scientists and engineers, the book describes various solutions spanning two to three orders of magnitude in pressure that have emerged in the past three decades. Many engineering concepts are illustrated through examples of real high pressure devices that have demonstrated their capacity and have produced scientific results.

After introducing basic engineering concepts related to the elastic and plastic behavior of cylindrical pressure devices, the text emphasizes mechanical and neutronic properties of construction materials. Subsequent chapters describe numerous high pressure techniques, including liquid/gas, clamp, and McWhan cells. The book also focuses on Paris-Edinburgh devices, high pressure metrology, and scientific applications.

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Zielgruppe


Researchers in materials physics, CMP, biophysics, geophysics, earth sciences, and chemistry.


Autoren/Hrsg.


Weitere Infos & Material


Basic Concepts

Basic elements of material strength

The cylindrical pressure vessel

Construction Materials I: Nonferrous Alloys

Copper beryllium
Titanium-zirconium (TiZr)
High tensile titanium alloys

High tensile aluminium alloys

Construction Materials II: Steels and Super-Alloys

General

The iron-carbon phase diagram

Other alloy elements

Designation (naming) of steels

High tensile steels

Stainless steels

Superalloys

Hydrogen compatibility

Construction Materials III: Sinter Materials

Tungsten carbide (TC)
Sintered cubic boron nitride (cBN)

Sintered diamond (SD)
Perspective: Nano-polycrystalline diamond (NPD)

Ceramics

Liquid/Gas and Clamp Pressure Cells
Liquid/gas pressure cells
Clamp cells

McWhan-Type Cells

General
Conclusion

Sapphire, Moissanite and Diamond Anvil Cells

Sapphire cells
Moissanite anvil cells (MACs)

Diamond anvil cells (DACs)

Special Designs

SANS high pressure cells

Single-crystal sapphire gas cells

Uniaxial Pressure Cells

General

Clamp devices

Remotely operated devices

Paris-Edinburgh Cells I

General

Load-frames

Anvils and gaskets
General remarks and observations

Paris-Edinburgh Cells II: Low and High Temperatures

General

Low temperatures
High temperatures

Paris-Edinburgh Cells III: Ancillary Equipment

Oil and gas compressors

Loading clamps

High pressure gas loading

Anvil rotor

Pressure Determination and Pressure Transmitting Media

Equations-of-state (EoS)

Pressure markers
Useful empirical rules

Pressure transmitting media (PTM)
General comments and recommendations

Applications

General

Diffraction
Inelastic scattering
Small angle neutron scattering (SANS)

Quasi-elastic neutron scattering (QENS)

Appendices
Bibliography
Index



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