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E-Book

E-Book, Englisch, 456 Seiten

Lacombe Adhesion Measurement Methods

Theory and Practice
Erscheinungsjahr 2010
ISBN: 978-1-4200-2882-9
Verlag: Taylor & Francis
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)

Theory and Practice

E-Book, Englisch, 456 Seiten

ISBN: 978-1-4200-2882-9
Verlag: Taylor & Francis
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)



Adhesion Measurement Methods: Theory and Practice provides practical information on the most important measurement techniques, their unique advantages and disadvantages, and the selection of the proper method for a given application. It includes useful information and formulae on adhesion related matters such as driving force formulae for various modes of delamination, methods for estimating stress buildup, and material property data in support of "back of the envelope" calculations.

The author presents optimal methods and tools used for measuring the adhesion of coatings and thin films as well as setting appropriate adhesion strength requirements. He provides a detailed overview of uses, implementation, and drawbacks for qualitative, semi-quantitative, and fully quantitative adhesion measurement techniques and self-loading systems. The book discusses thermal-mechanical behavior assessment, the application of the continuum theory of solids, and fracture mechanics, highlighting useful measures of adhesion strength such as stress intensity factor and strain energy release rate. It provides specific examples of how adhesion testing is carried out in practice, including the peel test, the scratch test, and the pull test, and describes the measurement of residual stress in a coating or other laminate structure. The book concludes with examples taken from the author's experience in the microelectronics industry and contains several appendices for looking up simple formulae and material property data for performing everyday calculations.

Adhesion Measurement Methods is an ideal addition for courses on materials science, mechanics of materials, or engineering design of laminate structures at the advanced undergraduate or graduate level.

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Zielgruppe


Scientists and technicians in R&D, manufacturing, processing, quality control, reliability, semiconductor fabrication, materials science, coatings technology, laminate and multilaminate structures, thin- and thick-films, aerospace engineering, and advanced undergraduate and graduate students in these areas.


Autoren/Hrsg.


Weitere Infos & Material


INTRODUCTION

Overview

What Is Adhesion and Can It Be Measured?
Definition A: Criteria for a Truly Useful Definition of the Term Adhesion
Definition B: Adhesion

Comments on Nomenclature and Usage

References

OVERVIEW OF MOST COMMON ADHESION MEASUREMENT METHODS

Preamble
Peel Test

Introduction

Advantages of the Peel Test

Disadvantages of the Peel Test

Summary and Recommendations

2.3 Tape Peel Test

Introduction

Advantages of the Tape Peel Test
Disadvantages of the Tape Peel Test

Summary and Recommendations

Pull Test
Introduction

Advantages of the Pull Test

Disadvantages of the Pull Test

Summary and Recommendations

Indentation Debonding Test

Introduction

Advantages of the Indentation Debonding Test

Disadvantages of the Indentation Debonding Test
Summary and Recommendations

Scratch Test

Introduction

Advantages of the Scratch Test

Disadvantages of the Scratch Test

Summary and Recommendations

Blister Test

Introduction

Advantages of the Blister Test
Disadvantages of the Blister Test

Summary and Recommendations

Beam-Bending Tests

Introduction

Three-Point Bend Test

Four-Point Bend Test

Standard Double Cantilevered Beam Test
Tapered Double Cantilevered Beam Test

Double-Cleavage Drilled Compression Test

Brazil Nut Test

Wedge Test

Topple Beam Test
Advantages of Beam-Bending Tests
Disadvantages of Beam-Bending Tests

Summary and Recommendations

Self-Loading Tests

Circle Cut Test

Modified Edge Liftoff Test

Microstrip Test

Advantages of Self-Loading Tests
Disadvantages of Self-Loading Tests

Summary and Recommendations

More Exotic Adhesion Measurement Methods
Laser Spallation: Early Work
Later Refined Experiments

Laser-Induced Decohesion Spectroscopy Experiment

Advantages of Laser Spallation Tests
Disadvantages of Laser Spallation Test
Summary and Recommendations

Electromagnetic Test

Advantages of the Electromagnetic Test

Disadvantages of the Electromagnetic Test
Summary and Recommendations

Nondestructive Tests

Dynamic Modulus Test

Advantages of the Dynamic Modulus Test

Disdvantages of the Dynamic Modulus Test
Summary and Recommendations

Surface Acoustic Waves Test

Advantages of the Surface Acoustic Waves Test

Disadvantages of the Surface Acoustic Waves Test

Summary and Recommendations

Notes

THEORETICAL FOUNDATIONS OF QUANTITATIVE ADHESION MEASUREMENT METHODS
Introduction to Continuum Theory
Concept of Stress in Solids
Special Stress States and Stress Conditions
Equation of Motion in Solids

Deformation and Strain
Constitutive Relations or Connecting the Stress to the Strain
Examples

Simple Deformations

Solving the Field Equations
Uniaxial Tension

Biaxial Tension
Triaxial Stress Case
Application to Simple Beams
General Methods for Solving Field Equations of Elasticity
Displacement Formulation

Stress Formulation

Mixed Formulation
Numerical Methods
Introduction

Detailed Stress Behavior of a Flexible Coating on a Rigid Disk
Strain Energy Principles

The Marvelous Mysterious J Integral
Summary

Notes

ELEMENTARY FRACTURE MECHANICS OF SOLIDS: APPLICATION TO PROBLEMS OF ADHESION
Introduction

Introductory Concepts
Fracture Mechanics as Applied to Problems of Adhesion
Elementary Computational Methods

Decohesion Number Approach of Suo and Hutchinson

Back-of-the-Envelope Calculations

Summary

Notes

APPLIED ADHESION TESTING
The Peel Test
Sample Preparation

Test Equipment

Peel Testing in Action
Advanced Peel Testing
Thermodynamics of the Peel Test

Deformation Calorimetry
Fully Quantitative Peel Testing
Earliest Work, Elastic Analysis
Elastic-Plastic Analysis

Full Elastic-Plastic Analysis

The Scratch/Cut Test
The Cut Test
Simplified Analytical Model for Cut Test

The Pull Test

Summary

Notes

ADHESION ASPECTS OF COATING AND THIN FILM STRESSES
Introduction

General Measurement Methods for Thin Films and Coatings

Cantilevered Beam Method

Variations on Bending Beam Approach

Optical Measurement of Deflection
X-ray Measurements

Ultrasonics
Photoelasticity

Strain Relief Methods

Magnetics

Raman Spectroscopy
Miscellaneous Methods
Summary

References

CASE STUDIES FROM THE FIELD

A Study in Adhesion Sensitivity to Contamination

Case of the Improperly Cured Film

Case of the Stressed Pin

Stability Maps

Summary

Notes

Appendix A: Vectors and Vector Calculus
Appendix B: Notes on Elementary Strength of Materials (SOM) Theory

Appendix C: Material Property Data for Selected Substances

Appendix D: Driving Force Formulae for a Variety of Laminate Structures

Appendix E: Selected References and Commentary on Adhesion Measurement and Film Stress Literature

Appendix F: General Adhesion Measurement References



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