Lawrence Trace Analysis

Volume 3
1. Auflage 2013
ISBN: 978-1-4832-6405-9
Verlag: Elsevier Science & Techn.
Format: PDF
Kopierschutz: 1 - PDF Watermark

E-Book, Englisch, 268 Seiten, Web PDF

Trace Analysis, Volume 3 focuses on critical discussions of selected topics in organic and inorganic analytical chemistry including instrumentation, techniques, and applications to the detection, identification, and quantitation of trace quantities of substances in a large variety of sample materials. The book is divided into two parts: Section 1, biological fluids and tissues, and Section 2, environmental analysis. Chapters are devoted in the discussion of subjects on the analysis of carbonyl compounds; the use of enzymatic methods for clinical analysis; the use of fluorescence spectroscopy for single compounds or multicomponent analysis of pollutants in air, water, and soils, with emphasis on fuel oils; and the analysis of polycyclic aromatic compounds in combustion emissions. Organic and inorganic chemists and medical technicians will find the book a good reference text.

Autoren/Hrsg.

Lawrence, James F.

Inhaltsverzeichnis

1;Front Cover;1
2;Trace Analysis;4
3;Copyright Page;5
4;Table of Contents;6
5;CONTRIBUTORS;8
6;PREFACE;10
7;CONTENTS OF PREVIOUS VOLUMES;12
8;Section 1: BIOLOGICAL FLUIDS AND TISSUES;14
8.1;CHAPTER 1. RECENT DEVELOPMENTS IN THE DETERMINATION OF CARBONYL COMPOUNDS IN BIOLOGICAL FLUIDS AND TISSUES;16
8.1.1;I. INTRODUCTION;16
8.1.2;II. NONCHROMATOGRAPHIC METHODOLOGIES;18
8.1.3;III. CHROMATOGRAPHIC METHODOLOGIES WITHOUT DERIVATIZATION;20
8.1.4;IV. CHROMATOGRAPHY OF DERIVATIZED COMPOUNDS;31
8.1.5;V. CONCLUSIONS;39
8.1.6;REFERENCES;39
8.2;CHAPTER 2. RECENT DEVELOPMENTS IN ENZYMATIC METHODS FOR CLINICAL ANALYSIS;44
8.2.1;I. INTRODUCTION;44
8.2.2;II. NEW TECHNIQUES IN CLINICAL ANALYSIS;52
8.2.3;III. COMMERCIAL INSTRUMENTS;78
8.2.4;REFERENCES;79
8.3;CHAPTER 3. CHLORINATED HYDROCARBON RESIDUES IN PRIMATE TISSUES AND FLUIDS;84
8.3.1;I. INTRODUCTION;84
8.3.2;II. MATERIALS;85
8.3.3;III. METHODOLOGY;87
8.3.4;REFERENCES;124
8.4;CHAPTER 4. ANALYSIS OF ASCORBIC ACID AND RELATED COMPOUNDS IN FLUIDS AND TISSUES;126
8.4.1;I. INTRODUCTION;126
8.4.2;II. CHEMICAL PROPERTIES OF ASCORBIC ACID AND ITS OXIDATION PRODUCTS;128
8.4.3;III. EXTRACTING ASCORBIC ACID AND DEHYDROASCORBIC ACID;130
8.4.4;IV. DETERMINATION OF ASCORBIC ACID, DEHYDROASCORBIC ACID, AND DIKETOGULONIC ACID;132
8.4.5;V. DETERMINATION OF COMPOUNDS RELATED TO ASCORBIC ACID;146
8.4.6;REFERENCES;147
8.5;CHAPTER 5. RECENT DEVELOPMENTS IN THERAPEUTIC DRUG MONITORING OF ANTIEPILEPTIC DRUGS;152
8.5.1;I. INTRODUCTION;152
8.5.2;II. CHROMATOGRAPHY;153
8.5.3;III. IMMUNOCHEMICAL ASSAYS;162
8.5.4;IV. CONCLUSIONS;167
8.5.5;REFERENCES;168
9;Section 2: ENVIRONMENTAL ANALYSIS;174
9.1;CHAPTER 6. DETERMINATION OF ENVIRONMENTAL POLLUTANTS BY DIRECT FLUORESCENCE SPECTROSCOPY;176
9.1.1;I. INTRODUCTION;176
9.1.2;II. BASIC ASPECTS;178
9.1.3;III. FLUORESCENCE SPECTROSCOPY;190
9.1.4;IV. OIL POLLUTION;195
9.1.5;V. OTHER APPLICATIONS;215
9.1.6;VI. CONCLUDING REMARKS;219
9.1.7;REFERENCES;221
9.2;CHAPTER 7. ANALYSIS OF POLYCYCLIC AROMATIC COMPOUNDS IN COMBUSTION EMISSIONS;226
9.2.1;I. INTRODUCTION;227
9.2.2;II. SAMPLE PREPARATION;228
9.2.3;III. GAS CHROMATOGRAPHY;237
9.2.4;IV. HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY;244
9.2.5;V. MASS SPECTROMETRY;249
9.2.6;VI. FLUORESCENCE AND PHOSPHORESCENCE;254
9.2.7;REFERENCES;261
10;INDEX;268