E-Book, Englisch, 282 Seiten, Web PDF
Sherma Advanced Analytical Techniques
1. Auflage 2013
ISBN: 978-1-4832-2094-9
Verlag: Elsevier Science & Techn.
Format: PDF
Kopierschutz: 1 - PDF Watermark
Analytical Methods for Pesticides and Plant Growth Regulators, Vol. 17
E-Book, Englisch, 282 Seiten, Web PDF
ISBN: 978-1-4832-2094-9
Verlag: Elsevier Science & Techn.
Format: PDF
Kopierschutz: 1 - PDF Watermark
Analytical Methods for Pesticides and Plant Growth Regulators, Volume XVII: Advanced Analytical Techniques covers analytical techniques of great importance to the pesticide analyst. The book discusses sampling techniques, universal extraction, cleanup methods, and cleanup by sweep co-distillation. The text also describes determinations by GC/FT-IR and GC/MS, computer evaluation of GC data, and immunoassay techniques for pesticide analysis. Toxicologists and people involved in pesticide analysis will find the book invaluable.
Autoren/Hrsg.
Weitere Infos & Material
1;Front Cover
;1
2;Advanced Analytical Techniques;4
3;Copyright Page;5
4;Table of Contents
;6
5;Preface;10
6;Chapter 1. Sampling Techniques for Pesticide Analysis;12
6.1;I. Introduction;12
6.2;II. Sampling Theory;16
6.3;III. Air Sampling for Pesticides;18
6.4;IV. Food and Crop Sampling;24
6.5;V. Soil Sampling;26
6.6;VI. Water Sampling;30
6.7;VII. Miscellaneous Sampling;39
6.8;References;40
7;Chapter 2. Universal Extraction and Cleanup Methods;46
7.1;I. Introduction;46
7.2;II. Universal Extraction Methods;48
7.3;III. Universal Cleanup Methods;72
7.4;IV. Internal Lab Control;82
7.5;References;82
8;Chapter 3. Sweep Codistillation: Recent Developments and Applications;86
8.1;I. Introduction;86
8.2;II. Equipment;87
8.3;III. Volatility Studies;91
8.4;IV. Pesticide Separation from Animal Fats;92
8.5;V. Pesticide Separation from Plant Material;101
8.6;VI. Miscellaneous Applications;106
8.7;VII. Interlaboratory Studies;107
8.8;VIII. New Developments;108
8.9;IX. Conclusions;109
8.10;References;109
9;Chapter 4. Pesticide Determination by GC/FT-IR Spectrometry;112
9.1;I. Introduction;112
9.2;II. Experimental Design;112
9.3;III. Advantages;114
9.4;IV. Applications;116
9.5;V. Residue Analysis;124
9.6;VI. Other FT-IR Interfaces;125
9.7;VII. Computer Methods of Analysis;126
9.8;VIII. Other Vibrational Techniques;127
9.9;References;127
10;Chapter 5. Application of Liquid Chromatography-Mass Spectrometry to the Determination of Pesticides;130
10.1;I. Introduction;130
10.2;II. LC-MS Interfaces;131
10.3;III. Application of Case Histories;144
10.4;IV. Summary;170
10.5;References;175
11;Chapter 6. Application of Computers for the Evaluation of Gas Chromatographic Data;178
11.1;I. Introduction;178
11.2;II. Instrumentation;180
11.3;III. Working with the Chromatography System;186
11.4;IV. Software for Pesticide Residue Analysis;191
11.5;V. Conclusion;220
11.6;VI. Appendix: Glossary of Terms;222
11.7;References;225
12;Chapter 7. Immunoassay Techniques for Pesticide Analysis;228
12.1;I. Introduction;228
12.2;II. Immunoassay Terminology;229
12.3;III. Steps in Immunoassay Development;231
12.4;IV. Benefits and Disadvantages of Monoclonal Antibodies;242
12.5;V. Applications of Pesticide Immunoassays;245
12.6;VI. Applying Immunoassays to Residue Analysis;252
12.7;VII. Implementation of Immunoassay Technology;263
12.8;VIII. Future Applications of Immunoassay Technology;266
12.9;IX. Conclusion;271
12.10;References;272
13;INDEX;276
