Sherma / Zweig Paper Chromatography

1. Auflage 2013
ISBN: 978-1-4832-8182-7
Verlag: Elsevier Science & Techn.
Format: PDF
Kopierschutz: 1 - PDF Watermark

E-Book, Englisch, 628 Seiten, Web PDF

Paper Chromatography and Electrophoresis, Volume II presents methods, techniques and complete experimental procedures in paper chromatography. The book provides information and applications of paper chromatography such as the theory, mechanism, and fundamentals of the process; the separation of amino acids, carbohydrates, lipophilic steroids, and related compounds; and the separation and estimation of inorganic ions by paper chromatography. Chemists and laboratory researchers and technicians will find the book a valuable reference material.

Autoren/Hrsg.

Sherma, Joseph

Zweig, Gunter

Inhaltsverzeichnis

1;Front Cover;1
2;Paper Chromatography;4
3;Copyright Page;5
4;Table of Contents;6
5;Preface;10
6;Contents of Volume I;12
7;Chapter 1. History and Introduction;16
7.1;I. History;16
7.2;II. Future Progress in Paper Chromatography;18
7.3;References;19
8;Chapter 2. Theory, Mechanism, and Fundamentals of Paper Chromatography;21
8.1;I. Introduction;21
8.2;II. Theory and Mechanism;23
8.3;III. RF and RM Values;29
8.4;IV. Artifacts and Anomalous Zones;36
8.5;References;42
9;Chapter 3. Techniques of Paper Chromatography;45
9.1;I. The Chromatography Laboratory;45
9.2;II. Sample Preparation;47
9.3;III. Sample Spotting;47
9.4;IV. The Paper;51
9.5;V. The Solvent;64
9.6;VI. Development;68
9.7;VII. Detection Methods;88
9.8;VIII. Qualitative Evaluation, Preservation, and Storage of Chromatograms;93
9.9;IX. Identification of Chromatographic Spots;95
9.10;X. Preparative Paper Chromatography;97
9.11;References;99
10;Chapter 4. Quantitative Paper Chromatography;105
10.1;I. Formation of the Colored Derivative;105
10.2;II. Estimation of the Spots;106
10.3;III. Sources of Error in Quantitative Paper Chromatography;120
10.4;References;123
11;Chapter 5. Amines, Amino Acids, Peptides, and Proteins;125
11.1;I. Aliphatic and Aromatic Amines;125
11.2;II. Amino Acids;135
11.3;III. Peptides;155
11.4;IV. Proteins;158
11.5;References;161
12;Chapter 6. Carbohydrates;167
12.1;I. Introduction;167
12.2;II. General Procedure;168
12.3;III. Miscellaneous Classes of Carbohydrates;178
12.4;References;184
13;Chapter 7. Aliphatic Acids;187
13.1;I. Preparation of Samples;187
13.2;II. Filter Paper;191
13.3;III. Solvents for Chromatographic Development;192
13.4;IV. Detection Reagents;206
13.5;V. Quantitative Analysis;210
13.6;References;211
14;Chapter 8. Steroids, Bile Acids, and Cardiac Glycosides;215
14.1;I. Steroids;215
14.2;II. Bile Acids and Other Steroid Acids;247
14.3;III. Cardiac Glycosides and Aglycones (Cardenolides, Bufadienolides);252
14.4;References;259
15;Chapter 9. Purines, Pyrimidines, and Related Compounds;263
15.1;I. Preparation of Samples;263
15.2;II. Detection and Identification;265
15.3;III. Methods and Techniques;269
15.4;IV. Chromatographic Systems;270
15.5;V. Quantitative Methods;272
15.6;VI. Applications;274
15.7;References;296
16;Chapter 10. Indoles, Phenols, and Aromatic Acids;298
16.1;I. Indoles;298
16.2;II. Phenols and Aromatic Acids;311
16.3;References;330
17;Chapter 11. Naturally Occurring Pigments;334
17.1;I. Fat-Soluble Chloroplast Pigments;334
17.2;II. Various Other Porphyrins;349
17.3;III. Flavonoids;356
17.4;References;365
18;Chapter 12. Pesticides;370
18.1;I. Introduction;370
18.2;II. Chlorinated Insecticides;372
18.3;III. Organophosphate Insecticides;378
18.4;IV. Carbamate Insecticides;390
18.5;V. Herbicides;394
18.6;VI. Fungicides;401
18.7;VII. Miscellaneous Pesticides and Related Products;403
18.8;VIII. Food and Feed Additives;406
18.9;References;410
19;Chapter 13. Antibiotics and Vitamins;412
19.1;I. Antibiotics;412
19.2;II. Vitamins;434
19.3;References;448
20;Chapter 14. Miscellaneous Organic Compounds;453
20.1;I. Hydrocarbons;453
20.2;II. Alcohols;457
20.3;III. Oxo Compounds;462
20.4;IV. Organic Peroxides;469
20.5;V. Nitro Compounds;472
20.6;VI. Alkaloids;475
20.7;VII. Synthetic Dyes;484
20.8;VIII. Sulfur Compounds;488
20.9;IX. Methylphenylpolysiloxanes;499
20.10;X. Phosphorus Compounds;499
20.11;XI. Epoxy Resins;509
20.12;References;509
21;Chapter 15. Inorganic Analysis;515
21.1;I. Cations;515
21.2;II. Common Anions;540
21.3;III. Miscellaneous Inorganic Substances;545
21.4;References;549
22;Author Index;554
23;Subject Index;588