Wasylishen / Ashbrook / Wimperis NMR of Quadrupolar Nuclei in Solid Materials

1. Auflage 2012
ISBN: 978-1-118-58885-7
Verlag: John Wiley & Sons
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)

E-Book, Englisch, 550 Seiten, E-Book

Reihe: eMagRes Books

The content of this volume has been added toeMagRes (formerly Encyclopedia of MagneticResonance) - the ultimateonline resource for NMR and MRI.
Over the past 20 years technical developments in superconductingmagnet technology and instrumentation have increased the potentialof NMR spectroscopy so that it is now possible to study a widerange of solid materials. In addition, one can probe the nuclearenvironments of many other additional atoms that possess theproperty of spin. In particular, it is possible to carry out NMRexperiments on isotopes that have nuclear spin greater that ½(i.e. quadrupolar nuclei). Since more that two-thirds of allNMR active isotopes are quadrupolar nuclei, applications of NMRspectroscopy with quadrupolar nuclei are increasing rapidly.
The purpose of this handbook is to provide under a single coverthe fundamental principles, techniques and applications ofquadrupolar NMR as it pertains to solid materials. Each chapter hasbeen prepared by an expert who has made significant contributionsto out understanding and appreciation of the importance of NMRstudies of quadrupolar nuclei in solids. The text is divided intothree sections: The first provides the reader with the backgroundnecessary to appreciate the challenges in acquiring andinterpreting NMR spectra of quadrupolar neclei in solids. Thesecond presents cutting-edge techniques and methodology foremploying these techniques to investigate quadrupolar nuclei insolids. The final section explores applications of solid-state NMRstudies of solids ranging from investigations of dynamics,characterizations of biological samples, organic and inorganicmaterials, porous materials, glasses, catalysts, semiconductors andhigh-temperature superconductors.
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Autoren/Hrsg.

Wasylishen, Roderick E.

Ashbrook, Sharon E.

Wimperis, Stephen

Inhaltsverzeichnis

Contributors ix
Series Preface xiii
Volume Preface xv
Part A Basic Principles
1 Quadrupolar Interactions
Pascal P. Man
2 Quadrupolar Nuclei in Solids
Alexander J. Vega
3 Quadrupolar Coupling: An Introduction and CrystallographicAspects
Sharon E. Ashbrook, Stephen Wimperis
4 Quadrupolar Nuclei in Solids: Influence of DifferentInteractions on Spectra
David L. Bryce, Roderick E. Wasylishen
Part B Advanced Techniques
5 Acquisition of Wideline Solid-State NMR Spectra of QuadrupolarNuclei
Robert W. Schurko
6 Sensitivity and Resolution Enhancement of Half-IntegerQuadrupolar Nuclei in Solid-State NMR
Thomas T. Nakashima, Roderick E. Wasylishen
7 Quadrupolar Nutation Spectroscopy
Arno P. M. Kentgens
8 Dynamic Angle Spinning
Philip J. Grandinetti
9 Double Rotation (DOR) NMR
Ray Dupree
10 MQMAS NMR: Experimental Strategies
Jean-Paul Amoureux, Marek Pruski
11 STMAS NMR: Experimental Advances
Sharon E. Ashbrook, Stephen Wimperis
12 Correlation Experiments Involving Half-Integer QuadrupolarNuclei
Michael Deschamps, Dominique Massiot
13 Computing Electric Field Gradient Tensors
Josef W. Zwanziger
Part C. Applications
14 Quadrupolar NMR to Investigate Dynamics in SolidMaterials
Luke A. O'Dell, Christopher I. Ratcliffe
15 Alkali Metal NMR of Biological Molecules
Gang Wu
16 Nitrogen-14 NMR Studies of Biological Systems
Luminita Duma
17 Oxygen-17 NMR Studies of Organic and BiologicalMolecules
Gang Wu
18 Oxygen-17 NMR of Inorganic Materials
Sharon E. Ashbrook, Mark E. Smith
19 Chlorine, Bromine and Iodine Solid-State NMR
David L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, RobertJ. Attrell
20 Quadrupolar NMR of Ionic Conductors, Batteries, and otherEnergy-Related Materials
Frédéric Blanc, Leigh Spencer, Gillian R.Goward
21 Quadrupolar NMR of Nanoporous Materials
Mohamed Haouas, Charlotte Martineau, Francis Taulelle
22 Quadrupolar NMR in the Earth Sciences
Jonathan F. Stebbins
23 Quadrupolar NMR of Superconductors
Nicholas J. Curro
24 Quadrupolar NMR of Semiconductors
James P. Yesinowski
25 Quadrupolar NMR of Metal Nuclides in BiologicalMaterials
Tatyana Polenova, Andrew S. Lipton, Paul D. Ellis
26 Nuclear Waste Glasses: Insights from Solid-State NMR
Scott Kroeker
27 Quadrupolar Metal NMR of Oxide Materials IncludingCatalysts
Olga B. Lapina, Victor V. Terskikh
28 Quadrupolar NMR of Intermetallic Compounds
Frank Haarmann
Index