Weisz / Belcher / Gordon Microanalysis by the Ring-Oven Technique

International Series of Monographs in Analytical Chemistry
2. Auflage 2013
ISBN: 978-1-4831-5330-8
Verlag: Elsevier Science & Techn.
Format: PDF
Kopierschutz: 1 - PDF Watermark

E-Book, Englisch, 180 Seiten, Web PDF

International Series of Monographs in Analytical Chemistry, Volume 37: Microanalysis by the Ring-Oven Technique, Second Edition focuses on the ring-oven method. The book first offers information on the characteristics and uses of ring-oven, gas generator, pipette, glass holder, and other accessories. The text focuses on qualitative analysis, including the systematic schemes for the analysis of metal ions; separations and reactions for acid radicals; and reactions for metal ions. The selection discusses spot colorimetry with the ring-oven method. Concerns include determination of iron and other metals, amplification reactions, removal of interfering ions, and determination of anions. The radiochemical applications of ring-oven method, including determination of inactive substances, identification of radionucleides, and separation procedures, are explained. The text also discusses the combination of ring-oven method with electrography, thin-layer chromatography, and solvent extraction. The book is a valuable source of information for readers interested in the ring-oven method.

Autoren/Hrsg.

Weisz, Herbert

Belcher, R.

Gordon, L.

Inhaltsverzeichnis

1;Front Cover;1
2;Microanalysis by The Ring-Oven Technique;4
3;Copyright Page;5
4;Table of Contents;6
5;FOREWORD;8
6;PREFACE;10
7;INTRODUCTION;12
8;CHAPTER I. THE APPARATUS AND ITS USE;16
8.1;A. THE RING OVEN;16
8.2;B. THE GAS GENERATOR;24
8.3;C. THE SAMPLE PIPETTE AND GLASS HOLDER;26
8.4;D. SOME ACCESSORIES;28
9;CHAPTER II. QUALITATIVE ANALYSIS;30
9.1;A. WITHOUT SEPARATIONS;30
9.2;B. SEPARATIONS;31
9.3;C. SYSTEMATIC SCHEMES FOR THE ANALYSIS OF METAL IONS;37
9.4;D. REACTIONS FOR METAL IONS;56
9.5;E. SEPARATIONS AND REACTIONS FOR ACID RADICALS;70
9.6;F. REAGENTS AND FILTER PAPER;78
10;CHAPTER III. SPOT COLORIMETRY WITH THE RING-OVEN METHOD, "RING COLORIMETRY";82
10.1;A. THE DETERMINATION OF IRON;85
10.2;B. THE DETERMINATION OF OTHER METALS;89
10.3;C. REMOVAL OF INTERFERING IONS;97
10.4;D. THE DETERMINATION OF SOME ANIONS;98
10.5;E. AMPLIFICATION REACTIONS;98
10.6;F. UNIVERSAL STANDARD SCALES;100
11;CHAPTER IV. ORGANIC SUBSTANCES;107
12;CHAPTER V. RADIOCHEMICAL APPLICATIONS;114
12.1;A. DETERMINATION OF ACTIVITIES;114
12.2;B. IDENTIFICATION OF RADIONUCLEIDES;122
12.3;C. SOME SPECIAL SEPARATION PROCEDURES;123
12.4;D. DETERMINATION OF INACTIVE SUBSTANCES;128
13;CHAPTER VI. THE RING-OVEN METHOD COMBINED WITH OTHER TECHNIQUES;130
13.1;A. RING-OVEN METHOD AND ELECTROGRAPHY;130
13.2;B. COMBINATION WITH PAPER- AND THIN-LAYER CHROMATOGRAPHY;135
13.3;C. COMBINATION WITH SOLVENT EXTRACTION;142
13.4;D. COMBINATIONS WITH OTHER TECHNIQUES;144
14;CHAPTER VII. APPLICATIONS IN VARIOUS FIELDS;146
14.1;A. AIR-POLLUTION STUDIES;147
14.2;B. TRACE ANALYSIS AND TOXICOLOGY;151
15;CHAPTER VIII. CONCENTRATION OF SUBSTANCES IN THE FORM OF A STRAIGHT LINE;154
16;CONCLUSION;156
17;APPENDIX;158
18;LIST OF ORIGINAL RING-OVEN PUBLICATIONS;160
19;REFERENCES;168
20;INDEX;176
21;OTHER TITLES IN THE SERIES IN ANALYTICAL CHEMISTRY;182