E-Book, Englisch, 240 Seiten
Lerner Small-Scale Synthesis of Laboratory Reagents with Reaction Modeling
Erscheinungsjahr 2011
ISBN: 978-1-4398-1313-3
Verlag: Taylor & Francis
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)
E-Book, Englisch, 240 Seiten
ISBN: 978-1-4398-1313-3
Verlag: Taylor & Francis
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)
The in-lab preparation of certain chemical reagents provides a number of advantages over purchasing various commercially prepared samples. This is especially true in isolated regions where acquiring the necessary substances from overseas can cause undue delay and inconvenience due to restrictions on the transportation of hazardous chemicals. An invaluable resource for chemists in a variety of environments, Small-Scale Synthesis of Laboratory Reagents with Reaction Modeling presents efficient, sensible, and versatile methods for the laboratory preparation of common chemical reagents.
Rapid, reliable synthesis
Designed to facilitate smooth experimentation in the lab, this volume presents preparations chosen for their short duration, availability of apparatus, high yield, and high purity of the product. Adding an educational component, the book also discusses fundamental processes in inorganic chemistry, presenting original modeling of reactions and their practical implementation. Theoretical aspects are discussed to a greater extent than is usual in synthetic literature in cases where there is a direct impact on experimental parameters, such as the reaction time, yield, and purity of the product.
More than 30 convenient, time-saving preparations
Focusing on simple synthesis of high-purity reagents, the book contains over 30 presentations, a substantial number of which are mathematically modeled for the first time. Most syntheses can be carried out in one day using common laboratory equipment, making this volume a valuable and time-saving tool.
Zielgruppe
Chemistry departments at universities and government and private research laboratories.
Autoren/Hrsg.
Fachgebiete
Weitere Infos & Material
Safety in the Laboratory
Sodium
Potassium
Lithium
Cesium
Lithium Hydride and Sodium Hydride
Bromine
Aluminum Bromide
Lithium Aluminum Hydride
Triethylaluminum and Diethylaluminum Bromide
Hydrazine Sulfate and Alcoholic Hydrazine Hydrate
Sodium and Potassium Azide
Potassium t-Butoxide and Potassium Hydride
Carbon Disulfide
Chlorine
Carbon Tetrachloride
Bis-Trichloromethyl Carbonate (Triphosgene)
Phosphorus Pentachloride
Phosphorus Oxychloride
Sulfur Trioxide and Oleum
Thionyl Chloride and Chlorosulfonic Acid
Appendix A: Assay of Reagents
Index