McDermott / Polenova Solid State NMR Studies of Biopolymers

1. Auflage 2012
ISBN: 978-1-118-58889-5
Verlag: John Wiley & Sons
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)

E-Book, Englisch, 592 Seiten, E-Book

The content of this volume has been added toeMagRes (formerly Encyclopedia of MagneticResonance) - the ultimate online resource for NMR and MRI.
The field of solid state NMR of biological samples [ssNMR] hasblossomed in the past 5-10 years, and a cohesive overview of thetechnology is needed for new practitioners in industry andacademia. This title provides an overview of Solid State NMRmethods for studying structure dynamics and ligand-binding inbiopolymers, and offers an overview of RF pulse sequences forvarious applications, including not only a systematic catalog butalso a discussion of theoretical tools for analysis of pulsesequences. Practical examples of biochemical applications areincluded, along with a detailed discussion of the many aspects ofsample preparation and handling that make spectroscopy on solidproteins successful.
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Autoren/Hrsg.

McDermott, Anne

Polenova, Tatyana

Inhaltsverzeichnis

Contributors.
Series Preface.
Volume Preface.
Part A: Fundamentals of Solid-State NMR Spectroscopy.
1 Internal Spin Interactions and Rotations in Solids (MichaelMehring).
2 Average Hamiltonian Theory (John S. Waugh).
3 Tensors inNMR (S. Chandra Shekar, Alexej Jerschow).
4 Chemical Shift Tensors (David M. Grant).
5 Magic Angle Spinning (E. Raymond Andrew).
6 Cross Polarization in Solids (Douglas P. Burum).
7 Quadrupolar Nuclei in Solids (Alexander J. Vega).
Part B: Recent Developments in Solid-State NMR Hardware andEmerging Methodologies for Structural and Dynamics Studies ofBiopolymers.
8 Probe Development for Biosolids NMR Spectroscopy (Peter L.Gor'kov, William W. Brey, Joanna R. Long).
9 High-Frequency Dynamic Nuclear Polarization (Melody L.Mak-Jurkauskas, Robert G. Griffin).
10 Homonuclear Dipolar Recoupling in Solid-State NMR (RobertTycko).
11 Dipolar Recoupling: Heteronuclear (Christopher P.Jaroniec).
12 Adiabatic Polarization-Transfer Methods in MAS Spectroscopy(Matthias Ernst, Beat H. Meier).
13 Symmetry-Based Pulse Sequences in Magic-Angle SpinningSolid-State NMR (Malcolm H. Levitt).
14 Dipolar-Based Torsion Angle Measurements for ProteinStructure Determination (Vladimir Ladizhansky).
15 Deuterated Peptides and Proteins: Structure and DynamicsStudies by MAS Solid-State NMR (Bernd Reif).
16 Correlation Spectroscopy for Resonance Assignments inSolid-State Proteins Using J-couplings (Leonard J. Mueller,Jeremy J. Titman).
17 Indirect Coupling and Connectivity (Anne Lesage).
18 Fast Magic-Angle Spinning for Protein Solid-State NMRSpectroscopy (Donghua H. Zhou).
19 Relaxation Studies of Solid Biopolymers (J´ozef R.Lewandowski, Lyndon Emsley).
Part C: Computational Aspects of Solid-State NMRSpectroscopy.
20 Proteins and Model Systems: Spectral Analyses (EricOldfield).
21 Numerical Simulations in Solid-State NMR with SIMPSON(Thomas Vosegaard, Zdencaronek Tocaronsner, Niels Chr.Nielsen).
22 Protein Structure Calculation Using Ambiguous Restraints(Michael Nilges, Th´er`ese Malliavin, BenjaminBardiaux).
23 Protein Structure Calculation and Automated NOE Restraints(Torsten Herrmann).
Part D: Applications of Solid-State NMR to Structural andDynamics Studies of Biopolymers.
24 Aligned Membrane Proteins: Structural Studies (Riqiang Fu,William W. Brey, Timothy A. Cross).
25 Membrane-Associated Systems: Structural Studies by MAS NMR(Christian Ader, Marc Baldus, Stefan Becker).
26 Structural Studies of Protein Fibrils and Misfolded Proteinsby Solid-State NMR (Beat H. Meier).
27 Structural and Dynamics Studies of Lipids by Solid-State NMR(Michele Auger).
28 REDOR Applications in Biology: An Overview (Orsolya Toke,Lynette Cegelski).
29 Quadrupolar Metal Nuclides in Bioinorganic Chemistry:Solid-State NMR Studies (Andrew S. Lipton, Tatyana Polenova,Paul D. Ellis).
30 Photosynthetic Antennae and Reaction Centers (Huub J. M.de Groot).
31 Structure and Function Studies of Energy and SignalTransducing Proteins by Solid-State NMR (Hideo Akutsu,Toshimichi Fujiwara).
32 Protein-Solvent Interactions in Solids (AnjaB¨ockmann).
33 Unifying Solution and Solid-State NMR Studies of Nucleic AcidDynamics (Kari Pederson, Dorothy C. Echodu, Prashant Emani, GregL. Olsen, Michael F. Bardaro Jr., Zahra Shajani, Gary A. Meints,Paul A. Miller, Gabriele Varani, Gary P. Drobny).
Index.