Tuzimski / Sherma High Performance Liquid Chromatography in Pesticide Residue Analysis

1. Auflage 2015
ISBN: 978-1-4665-6882-2
Verlag: Taylor & Francis
Format: PDF
Kopierschutz: Adobe DRM (»Systemvoraussetzungen)

E-Book, Englisch, 582 Seiten

Reihe: Chromatographic Science Series

HPLC is the principal separation technique for identification of the pesticides in environmental samples and for quantitative analysis of analytes. At each stage of the HPLC procedure, the chromatographer should possess both the practical and theoretical skills required to perform HPLC experiments correctly and to obtain reliable, repeatable, and reproducible results.

Developed to serve as a detailed practical guide, High Performance Liquid Chromatography in Pesticide Residue Analysis is a comprehensive source of information and training on state-of-the-art pesticide residue methods performed with the aid of HPLC. The book presents the pros and cons of HPLC as a flexible and versatile separation and analysis tool with multiple purposes and advantages in investigations of pesticides for food and plant drugs standardization, promotion of health, protection of new herbal medicines, and more.

Autoren/Hrsg.

Tuzimski, Tomasz

Sherma, Joseph

Fachgebiete

• Geowissenschaften Umweltwissenschaften Umweltwissenschaften
• Naturwissenschaften Chemie Analytische Chemie
• Naturwissenschaften Biowissenschaften Botanik

Inhaltsverzeichnis

Part I GENERAL ASPECTS

Overview of the field of chromatographic methods of pesticide residues analysis and organization of the book
Tomasz Tuzimski and Joseph Sherma

Pesticides classification and properties
Tomasz Tuzimski and Joseph Sherma

Method development of chromatography: Retention–eluent composition relationships. Application to analysis of pesticides
Edward Soczewinski

Choice of the mode of chromatographic method to analysis of pesticides on the basis of the properties of analytes
Piotr Kawczak, Tomasz Baczek, and Roman Kaliszan

Choice of the mode of sample preparation in the analysis of pesticides on the basis of the properties of the matrix
Robert Smith, Kevin Tran, Chris Sack, and Kristy Richards

Selection of the mode of stationary phases and columns to analysis of pesticides
Boguslaw Buszewski and Szymon Bocian

Selection of the type of mobile phases to analysis of nonionic analytes: reversed and normal-phase HPLC
Tomasz Tuzimski

Selection of the mobile phases to analysis of ionic analytes: reversed-phase, ion-pair, ion-exchange, ion-exclusion HPLC
Monika Waksmundzka-Hajnos, and Anna Petruczynik

Optimization of NP and RP systems for analysis of pesticides. Choice of the mode of elution - isocratic and gradient elution
Pavel Jandera

Part II

Kinetics study of pesticides in the environment: Application of HPLC to kinetics products of pesticides analyses. Lukasz Ciesla

Photochemical degradation of pesticides in the environment
Davide Vione

Part III

Sample preparation for determination of pesticides by HPLC
Robert Smith, Kevin Tran, Chris Sack, and Kristy Richards

Quantitative analysis. Method validation
Renato Zanella

Analysis of pesticides by HPLC-UV, HPLC-DAD (HPLC-PAD) and other detection methods
Tomasz Tuzimski

HPLC-MS as a method of identification and quantification of pesticides
Yolanda Picó

Multidimensional liquid chromatography applied to analysis of pesticides
Tadeusz Gorecki and Heba Shaaban

Chiral separation of some classes of pesticides by HPLC method
Hassan Y. Aboul-Enein

Application of chemiluminescence detection in analysis of pesticides by HPLC
Peipei Pan

UPLC applied to analysis of pesticides
María de los Ángeles Herrera Abdo, José Luis Martínez Vidal, and Antonia Garrido Frenich

HPLC versus other modern analytical methods for determination of pesticides
Tomasz Tuzimski and Joseph Sherma