Wang / Zhu / Xu Residual Stresses and Nanoindentation Testing of Films and Coatings

1. Auflage 2018
ISBN: 978-981-10-7841-5
Verlag: Springer Singapore
Format: PDF
Kopierschutz: 1 - PDF Watermark

E-Book, Englisch, 215 Seiten, eBook

This book covers the basic principles and application of nanoindentation technology to determine residual stresses in films and coatings. It briefly introduces various detection technologies for measuring residual stresses, while mainly focusing on nanoindentation. Subsequently, nanoindentation is used to determine residual stresses in different types of films and coatings, and to describe them in detail. 
This book is intended for specialists, engineers and graduate students in mechanical design, manufacturing, maintenance and remanufacturing, and as a guide to the practice of production with social and economic benefits.

Haidou Wang, Ph. D. is a Professor and his main research interests are in surface engineering and remanufacturing. His work focuses on the characterization and evaluation of surface coatings and films, including their mechanical properties, tribological properties and lifecycle evaluation. Haidou Wang is supported by the National Natural Science Foundation for Distinguished Young Scholars. He is the Chief Scientist of the National Defense 973 Program and the Fund Manager of the Key Program of National Natural Science Foundation and major program of National Natural Science Foundation of Beijing. 
His contributions have been recognized with a wealth of awards. He has published eight books in Chinese and English, 160 papers indexed by SCI, and 250 papers indexed by EI. In addition, he holds three American patents, 25 Chinese patents and 23 intellectual property rights patents.
Lina Zhu, Ph.D. is a Lecturer, and her main research interests are in surface engineering and tribology. Her work focuses on the characterization and evaluation of surface coatings and films, including the mechanical properties, tribological properties and wettability. Lina Zhu is supported by the National Natural Science Foundation and Natural Science Foundation of Beijing. She has published two books in Chinese, 25 papers indexed by the SCI, and 31 papers indexed by EI. In addition, she holds eleven Chinese patents. 
Binshi Xu is a member of the Chinese Academy of Engineering (CAE). He has been engaged in maintenance engineering, surface engineering and remanufacturing engineering for many years, and is one of the pioneers of surface engineering and remanufacturing engineering in China. Xu has carried out more than 80 projects, and has published seventeen books and more than 800 papers. In addition, he holds 20 patents. In 1996, he won the Center for Middle Eastern Studies (CMES) S&T Achievement Award; in 2004, he won the CAE's Guanghua Engineering Award. 

Zielgruppe

Research

Autoren/Hrsg.

Wang, Haidou

Zhu, Lina

Xu, Binshi

Inhaltsverzeichnis

1;Preface;5
2;About the Book;7
3;Contents;8
4;1 Residual Stresses of Materials;12
4.1;1.1 Definition and Classification of Residual Stresses;12
4.2;1.2 Formation Mechanism of Residual Stress;13
4.2.1;1.2.1 Formation Mechanism of Macroscopic Residual Stress;13
4.2.2;1.2.2 Formation Mechanism of Microscopic Residual Stress;14
4.3;1.3 Effect of Residual Stress on Properties of Materials;14
4.3.1;1.3.1 Effect of Residual Stress on Fatigue Strength;14
4.3.2;1.3.2 Effect of Residual Stress on Brittle Failure;15
4.3.3;1.3.3 Effect of Residual Stress on Stress Corrosion Cracking;16
4.3.4;1.3.4 Effect of Residual Stress on Machining Precision and Dimension Stability;17
4.4;1.4 Test Methods of Residual Stress;18
4.4.1;1.4.1 Nondestructive Testing Methods;18
4.4.1.1;1.4.1.1 X-ray Diffraction Method;18
4.4.1.2;1.4.1.2 Neutron Diffraction Method;19
4.4.1.3;1.4.1.3 Raman Spectroscopy Method;20
4.4.1.4;1.4.1.4 Ultrasonic Method;21
4.4.1.5;1.4.1.5 Magnetic Method;22
4.4.1.6;1.4.1.6 Synchrotron Radiation Method;23
4.4.2;1.4.2 Destructive Testing Methods;24
4.4.2.1;1.4.2.1 Hole Drilling Method;24
4.4.2.2;1.4.2.2 Stripping Method;25
4.4.2.3;1.4.2.3 Ring Core Method;25
4.4.2.4;1.4.2.4 Sectioning Method;26
4.4.2.5;1.4.2.5 Cutting Groove Method;28
4.5;References;28
5;2 Principle and Methods of Nanoindentation Test;31
5.1;2.1 Overview of Nanoindentation Technique;31
5.2;2.2 Measurement Principles of Hardness and Elastic Modulus;32
5.2.1;2.2.1 Oliver and Pharr Method (O&P Method);32
5.2.2;2.2.2 Work-of-Indentation Method;35
5.2.3;2.2.3 Continuous Stiffness Measurement;37
5.3;2.3 Nanoindentation Testing Method;38
5.3.1;2.3.1 Indenter Types;38
5.3.2;2.3.2 Nanoindentation Instrumentation;40
5.4;2.4 Factors Affecting Nanoindentation Test Results;45
5.5;References;46
6;3 Theoretical Models for Measuring Residual Stress by Nanoindentation Method;47
6.1;3.1 Principle of Measuring Residual Stress by Nanoindentation Method;47
6.2;3.2 Effect of Residual Stress on Nanoindentation Parameters [5];47
6.2.1;3.2.1 Effect of Residual Stress on Load–Depth Curves;49
6.2.2;3.2.2 Effect of Residual Stress on Pile-up Deformation;52
6.2.3;3.2.3 Effect of Residual Stress on Contact Area;57
6.2.4;3.2.4 Effect of Residual Stress on Mechanical Properties;58
6.3;3.3 Models for Measuring Residual Stress;59
6.3.1;3.3.1 Suresh Model;61
6.3.2;3.3.2 Lee Model;69
6.3.2.1;3.3.2.1 Lee Model I;69
6.3.2.2;3.3.2.2 Lee Model II;70
6.3.3;3.3.3 Xu Model;72
6.3.4;3.3.4 Swadener Model;73
6.3.4.1;3.3.4.1 Swadener Model I;73
6.3.4.2;3.3.4.2 Swadener Model II;74
6.4;3.4 Indentation Fracture Technique;75
6.5;References;76
7;4 Application of Suresh and Lee Models in the Measurement of Residual Stress of Bulk Materials;78
7.1;4.1 Measurement of Residual Stresses in Single Crystal Copper;78
7.1.1;4.1.1 Pile-up of Single Crystal Copper;78
7.1.2;4.1.2 Model Construction of the Real Contact Area;79
7.1.3;4.1.3 Comparison of Different Methods for Calculating Contact Area;82
7.1.4;4.1.4 The Real Contact Area of the Single Crystal Copper;84
7.1.5;4.1.5 The Real Hardness of the Single Crystal Copper;85
7.1.6;4.1.6 Residual Stress Calculation of the Single Crystal Copper;87
7.2;4.2 Residual Stress Determination of 1045 Steel;88
7.2.1;4.2.1 Experimental;88
7.2.2;4.2.2 Load–Depth Curves of the 1045 Steel;89
7.2.3;4.2.3 Pile-up Deformation of the 1045 Steel;89
7.2.4;4.2.4 The Real Hardness of the 1045 Steel;92
7.2.5;4.2.5 Calculation of Residual Stresses of the 1045 Steel;96
7.3;References;106
8;5 Application of Suresh and Lee Models in the Measurement of Residual Stress of Coatings;107
8.1;5.1 Residual Stresses of Fe-Based Laser Cladding Coatings;107
8.1.1;5.1.1 Preparation of Fe-Based Laser Cladding Coatings;107
8.1.2;5.1.2 Microstructures of Fe-Based Laser Cladding Coatings;109
8.1.3;5.1.3 Residual Stress Analysis of Fe-Based Laser Cladding Coatings;113
8.2;5.2 Residual Stress of Fe-Based Coatings Prepared by Supersonic Plasma Spraying;122
8.2.1;5.2.1 Preparation of Sprayed Fe-Based Coatings;122
8.2.2;5.2.2 Microstructure of Sprayed Fe-Based Coatings;123
8.2.3;5.2.3 Residual Stress Analysis of Sprayed Fe-Based Coatings;127
8.3;5.3 Residual Stress of Plasma Cladding Coatings;137
8.3.1;5.3.1 Preparation of Plasma Cladding Coatings;137
8.3.2;5.3.2 Microstructure of Plasma Cladding Coatings;138
8.3.3;5.3.3 Mechanical Properties of Plasma Cladding Coatings;140
8.3.4;5.3.4 Residual Stress Analysis of Plasma Cladding Coatings;142
8.4;5.4 Residual Stress of n-Al2O3/Ni Composite Brush Plating Coatings;146
8.4.1;5.4.1 Preparation of n-Al2O3/Ni Composite Brush Plating Coatings;147
8.4.2;5.4.2 Microstructure of n-Al2O3/Ni Composite Brush Plating Coatings;147
8.4.3;5.4.3 Mechanical Properties of n-Al2O3/Ni Composite Brush Plating Coatings;149
8.4.4;5.4.4 Residual Stress Analysis of n-Al2O3/Ni Composite Brush Plating Coatings;151
8.5;References;153
9;6 Application of Suresh and Lee Models in the Measurement of Residual Stress of Films;155
9.1;6.1 Residual Stress of Magnetron Sputtering Cu Films;155
9.1.1;6.1.1 Preparation of Magnetron Sputtering Cu Films;155
9.1.2;6.1.2 Microstructure of Magnetron Sputtering Cu Films;156
9.1.3;6.1.3 Mechanical Properties of Magnetron Sputtering Cu Films;160
9.1.4;6.1.4 Residual Stress Analysis of Magnetron Sputtering Cu Films;160
9.2;6.2 Residual Stress of Magnetron Sputtering Ti Films [4, 5];164
9.2.1;6.2.1 Preparation and Characterization of Magnetron Sputtering Ti Films;164
9.2.2;6.2.2 Effects of Process Parameters on the Hardness and Elastic Modulus of Ti Films;174
9.2.3;6.2.3 Effect of Process Parameters on the Residual Stress of Ti Films;180
9.3;6.3 Residual Stress of TiN Films and Ti/TiN Multilayer Films [6];186
9.3.1;6.3.1 Preparation and Characterization of TiN Films;186
9.3.2;6.3.2 Preparation and Characterization of Ti/TiN Multilayer Films;189
9.3.3;6.3.3 Hardness and Elastic Modulus of Ti/TiN Multilayer Films [7];191
9.3.4;6.3.4 Residual Stress Analysis of TiN and Ti/TiN Multilayer Films;194
9.4;References;198
10;7 Application of Other Models in the Measurement of Residual Stress;199
10.1;7.1 Application of the Xu Model;199
10.2;7.2 Application of the Swadener Model;201
10.2.1;7.2.1 Measurement of Surface Residual Stresses in SiC Particle-Reinforced Al Matrix Composites;201
10.2.2;7.2.2 Measurement of Residual Stresses in Cu and Cr Films;204
10.2.2.1;7.2.2.1 Cu Films;204
10.2.2.2;7.2.2.2 Cr Films;206
10.3;7.3 Application of Indentation Fracture Method;208
10.3.1;7.3.1 Measurement of Residual Stresses in Three-Layer Reaction Bonded Alumina Composites;208
10.3.2;7.3.2 Measurement of Residual Stresses in Soda-Lime Glass;210
10.3.3;7.3.3 Measurement of Residual Stresses in Lithium Disilicate Glass-Ceramic;212
10.4;References;215

Residual stresses of materials.- Principle and Methods of Nanoindentation Test.- Theoretical models for measuring residual stress by nanoindentation method.- Application of Suresh and Lee models in the measurement of residual stress of bulk materials.- Application of Suresh and Lee models in the measurement of residual stress of coatings.- Application of Suresh and Lee models in the measurement of residual stress of films.- Application of other models in the measurement of residual stress.

Über Autor(innen)

Haidou Wang, Ph. D. is a Professor and his main research interests are in surface engineering and remanufacturing. His work focuses on the characterization and evaluation of surface coatings and films, including their mechanical properties, tribological properties and lifecycle evaluation. Haidou Wang is supported by the National Natural Science Foundation for Distinguished Young Scholars. He is the Chief Scientist of the National Defense 973 Program and the Fund Manager of the Key Program of National Natural Science Foundation and major program of National Natural Science Foundation of Beijing.  His contributions have been recognized with a wealth of awards. He has published eight books in Chinese and English, 160 papers indexed by SCI, and 250 papers indexed by EI. In addition, he holds three American patents, 25 Chinese patents and 23 intellectual property rights patents. Lina Zhu, Ph.D. is a Lecturer, and her main research interests are in surface engineering and tribology. Her work focuses on the characterization and evaluation of surface coatings and films, including the mechanical properties, tribological properties and wettability. Lina Zhu is supported by the National Natural Science Foundation and Natural Science Foundation of Beijing. She has published two books in Chinese, 25 papers indexed by the SCI, and 31 papers indexed by EI. In addition, she holds eleven Chinese patents.  Binshi Xu is a member of the Chinese Academy of Engineering (CAE). He has been engaged in maintenance engineering, surface engineering and remanufacturing engineering for many years, and is one of the pioneers of surface engineering and remanufacturing engineering in China. Xu has carried out more than 80 projects, and has published seventeen books and more than 800 papers. In addition, he holds 20 patents. In 1996, he won the Center for Middle Eastern Studies (CMES) S&T Achievement Award; in 2004, he won the CAE’s Guanghua Engineering Award.